KOBASHI 橙花（苦橙花）精油 100%純淨天然

這是我們擁有過品質最頂級的橙花精油。

【拉丁學名】Citrus aurantium amara bigarade
【萃取方式】採用水蒸氣蒸餾法，從苦橙樹的花朵中萃取。獨特萃取工藝保留了精油的純淨與活性成分。
【顏色】清透淡黃
【產地】突尼斯—來自一座百年有機栽培老果園的頂尖品質。接下來的批次則來自西班牙值得信賴的供應商。
【香氣】精緻花香，帶有甜潤堅果與青草香調，異國風情濃郁迷人。

【產品亮點】

橙花精油被譽為放鬆心靈的完美伴侶，帶來舒緩、鎮靜效果，還被傳說有助於甜美夢境。對女性朋友特別友好，常被用於紓緩生理期不適與更年期相關症狀。對成熟與乾燥肌膚有極佳的護膚功效，能滋養肌膚並讓肌膚重現光彩。此精油濃郁珍貴，每375公斤花瓣僅能萃取約1公斤高品質精油，產量稀少，是市場上的珍品。

【歷史傳承】

苦橙花作為古老的珍稀香料，自中世紀以來就被廣泛種植與用於高級香水配方中。其獨特的芳香調令它成為香水調配的靈魂元素，亦經常被用以提升酒類飲品的風味。

【植物描述】

苦橙樹屬芸香科，為常綠喬木，高達十米，披覆濃密的深綠色葉片，盛開潔白芳香的花朵。原生於亞洲，現多生長於地中海地區及世界部分地區，喜歡乾燥氣候。

【真品保證】

市場上有大量劣質或合成橙花精油混淆視聽，但我們堅持只選購100%純天然橙花精油，並通過GC-MS分析確保品質純正，拒絕任何化學合成品。選擇KOBASHI，享受頂級純淨奢華芳香體驗，呵護身心，展現自然光彩。

KOBASHI NEROLI BIGARADE OIL 
100% Pure- AKA bitter Orange Blossom.

LATIN NAME: Citrus aurantium amara bigarade

SOURCE: Hydro-steam distilled from the flowers of the bitter orange tree. Neroli has to be extracted buy hydro steam distilling. If you don't place in water in the vessel, like all flowers, it would be turned in a waxy mass of sludge and you wouldn't get the steam through it.

COLOUR: Clear pale yellow.
ORIGIN: Tunisia from a small orchard of mature organically grown trees of early 1900's.
From the bitter orange top quality perfumery varieties, such as Bigarade Bouquet (riche depouille), Bigarade bouquetier à Grande fleurs and dwarfs. Distiller said, flowers are from trees that were planted by a French Man during colonisation. Tunsian only available in 1ml, the next batch is from our trusted supplier in Spain.

Density: 0.870

AROMA: exquisite light floral, sweet, slight nutty under tone, characteristic of the fresh flowers

True 100% Neroli Citrus aurantium amara bigarade, (bigaradia) commonly known as the bitter, sour or Seville orange. Neroli is mainly from Morocco, Spain and Tunisia. other origins are Egypt, Sicily, Haiti, France, Brazil and USA. There is only 800 to 1200 kg produced a year. Fresh flowers yielded approximately 0.28%. Around 375 kg of petals creates approximately 1 kg or less of quality oil. (1 kg of flowers yields can produce about 1g bigarade oil, but many factors dictate yield.)

Warning from my supplier distiller for next year's kg price: " Another thing you are missing is that for the same oil profile I sold you this year, I received offers to sell it for USD 10,000 at wholesale price for next year."

There are thousands of essential oil and perfume companies. We only purchased 3kgs this time. If we were to do the maths at the lowest calculations there is much more Neroli being sold than is physically being grown and distilled.

Of course I can't give an exact amount, but IMO 95% of the companies selling what they call Neroli is a chemical concoction.

It is easy for a chemist to manufacture a blend of aroma chemicals (naturally or synthetically derived) and call it what ever they want.

The public will not know the difference without a good noise and in depth Gc-MS analysis by an expert.

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QUALITIES: Antidepressant. calming and soothing during times of stress , helps restore sleep. Ideal for skin care, especially mature/dry types.

Used as an ingredient in eau de cologne and perfume: An ingredient in one of our luxury creams. We also have a hydrolat ( floral water) of neroli which is wonderful as a skin toner and conditioner. One kilo of blossoms yields about 1 ml of oil.

Not to be mistaken for the cheaper orange blossom oil which does not have the nutty flavour.

A member of the Rutaceae family, an evergreen tree up to ten metres high, with glossy dark green oval leaves. It has white fragrant flowers. Native to Asia but grows well in the Mediterranean

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{Between April and aug 2006 and May 2016 to July 2017 we did not supply Neroli due to not finding a suitable quality. }


Most Neroli on the market now is being adulterated by adding LIMONENE, LINALOOL, LINALYL ACETATE, a-TERPINEOL, GERANYL ACETATE,NEROL, GERANIOL, NEROLIDOL, METHYL ANTHRANILATE.

Linalool Natural sells at USD 30-00 kilo, Limonene Natural at USD 2-50 kilo, Alpha Pinene at pennies.
Put them all together and you got a very profitable situation.
Naphalene perfume catalyst) (should be 0%), Benzyl alcohol (should be 0%), and ethanol showing it is a pretty bad concoction, waste of time.}
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ANALYSIS

Product Name : NEROLI OIL

Aceite esencial de Neroli
Botanical name : Citrus aurantium
Origin : Spain

Analysis features :

Agilent GC System 7890A - Column : HP INNOWAX polaire : 60 m ´ 0,25 mm ´ 0,5 ul
Temperature program : 8 min to 95 °C - 4 °C/min till 190 °C - 29 min to 190ºC
Carrier gas H2 : 30 psis/FID. Injector : split. Sample : 0.1 ul without dilution
The compounds of the essential oils are identified by retention times.
% Are calculated from the peak areas given by the GC / FID without the use of a correction factor.

Physical characteristics:
Production date: May 2020
Density at 20°C 0,870
Refractive index at 20°C 1,470
Optical rotation at a 20°C 7,6

Kobashi's present Batch Sample Name: Neroli, 170607 Tunisia
Analysis by Pyrenessences

Date of reception : 06/14/2017 Date analysis : 06/15/2017
Packaging : Brown flask of 5 ml - ambient temperature
Wanted analysis : Classic analysis


- CPG 6890 / MS 5973 AGILENT - Column : VF WAX polar 60 m 0,25 mm 0,5 µm
- CPG 6890 FID AGILENT - Column : VF WAX polar 60 m 0,25 mm 0,5 µm
- Program : 6 min to 60°C - 2°C/min 250°C - 10 min to 250°C

- Carrier gas : He 30 psi/FID ; 23 psi/MS
- Dilution: 10 % in Hexane
- Mass : 30 à 350
- Sample injection : 1 µL

When the oils are tested the analyst has to dilute in hexane, pentane or acetone to be able to put it through the Gc-Ms columns. You can't run samples neat, as the detectors are very sensitive and the chemicals would overlap.

Mass range : 30 to 350, Oil components are identified by a combination of retention times (our own database) and mass spectra library NIST 75 000 records,
Percentages are calculated from GC/FID peaks areas without using corrections factors.

Naturally occurring in Neroli oil.
Peak RT (min) Compound %
1 4,0 ACETONE 0.01
2 6,0 TRICYCLENE 0.01
3 6,2 a-PINENE 0.62
4 6,3 a-THUYENE 0.03
5 7,3 CAMPHENE 0.05
6 8,4 b-PINENE 9.97
7 8,8 SABINENE 1.11
8 9,7 D3-CARENE 0.01
9 10,2 b-MYRCENE 1.66
10 10,3 y-LIMONENE 0.01
11 10,9 a-TERPINENE 0.07
12 11,8 LIMONENE 6.03
13 12,1 b-PHELLANDRENE + 1,8-CINEOLE 0.24
14 12,2 Cis-ARBUSCULON 0.02
15 13,3 Cis-b-OCIMENE 0.63
16 13,6 Trans ARBUSCULON 0.01
17 13,8 g-TERPINENE 0.12
18 14,1 Trans-b-OCIMENE 4.17
19 15,0 p-CYMENE 0.05
20 15,1 HEXYL ACETATE 0.01
21 15,7 TERPINOLENE 0.32
22 17,0 1,3,7-NONATRIENE, 4,8-DIMETHYL- 0.04
23 18,0 LINALOOL METHYL ETHER 0.01
24 18,6 5-HEPTEN-2-ONE, 6-METHYL- 0.02
25 19,4 1-HEXANOL 0.01
26 20,8 ALLO-OCIMENE 0.01
27 22,1 OXYDE D’a-PINENE 0.01
28 22,4 ANISALDEHYDE TRIMETHYL 0.01
29 22,6 TERPENIC KETONE 0.02
30 24,8 LINALOOL Cis-OXIDE 0.21
31 26,2 Trans-THUYANOL 0.02
32 26,5 LINALOOL trans-OXIDE 0.1
33 26,6 d-ELEMENE 0.03
34 2,0 OCTYL ACETATE 0.01
35 27,6 BICYCLOELEMENE 0.01
36 29,1 CAMPHOR 0.01
37 29,7 BENZALDEHYDE 0.03
38 31,6 LINALOOL 42.5
39 31,7 DIMETHYL SULFOXYDE 0.02
40 32,2 LINALYL ACETATE 13.37
41 32,4 Trans-p-MENTH-2-EN-1-OL 0.03
42 33,3 BORNYL ACETATE 0.02
43 33,5 FENCHOL 0.01
44 33,9 b-ELEMENE 0.01
45 34,3 b-CARYOPHYLLENE 0.34
46 34,6 TERPINENE-4-OL 0.33
47 35,2 HOTRIENOL 0.01
48 35,3 LINALYL PROPIONATE 0.03
49 35,5 MYRTENAL 0.02
50 36,2 Cis-p-MENTH-2-EN-1-OL 0.02
51 36,9 BENZENEACETALDEHYDE 0.01
52 37,0 GERMACRENE A 0.02
53 37,6 Trans-PINOCARVEOL 0.02
54 38,1 1-NONANOL 0.01
55 38,3 CITRONELLYL ACETATE 0.01
56 38,5 a-HUMULENE 0.04
57 38,6 E-b-FARNESENE 0.06
58 39,3 NERAL 0.01
59 40,2 TERPENYL ACETATE 0.13
60 40,3 a-TERPINEOL 4.8
61 40,8 HEPTADECANE 0.02
62 40,9 GERMACRENE D 0.06
63 41,7 a-MUUROLENE 0.04
64 42,1 NERYL ACETATE 1.39
65 42,2 GERANIAL 0.05
66 42,3 BICYCLOGERMACRENE 0.1
67 43,1 Cis-PIPERITOL 0.01
68 43,4 a-FARNESENE 0.04
69 43,8 GERANYL ACETATE 2.58
70 44,1 CITRONELLOL 0.02
71 44,3 b-SESQUIPHELLANDRENE 0.02
72 46,7 NEROL 1.07
73 47,0 2-PHENYLETHYL ACETATE 0.09
74 47,6 E,E-3,5,7-OCTATRIENE-2-OL, 2,6-DIMETHYL- 0.04
75 48,0 GERMACRENE B 0.02
76 48,9 GERANIOL 2.75
77 49,3 E-GERANYLACETONE 0.02
78 52,2 PHENYLETHYLIC ALCOHOL 0.03
79 53,0 PHENYL ACETONITRILE 0.15
80 53,9 Trans-JASMONE 0.02
81 54,3 2,6-DIMETHYL-3,7-OCTADIENE-2,6-DIOL 0.02
82 56,0 CARYOPHYLLENE OXIDE 0.01
83 58,8 PENTADECANAL 0.02
84 59,3 NEROLIDOL 1.98
85 62,9 PHENYLETHYLIC ESTER 0.04
86 63,3 PENTADECANONE TRIMETHYL 0.01
87 66,7 AROMATIC COMPONENT 0.02
88 67,7 CARVACROL 0.02
89 68,7 METHYL ANTHRANILATE 0.26
90 70,2 FARNESYL ACETATE 0.06
91 70,9 DITERPENE Mw=272 0.02
92 72,3 TRICOSANE 0.04
93 72,5 FARNESOL ISOMER 0.01
94 74,4 Trans,trans-FARNESOL 1.15
95 78,0 INDOLE 0.22
96 81,3 PENTACOSANE 0.02
97 83,0 METHYL-N-FORMYLANTHRANILATE 0.01
98 85,7 PHYTOL 0.01
99 89,6 HEPTACOSANE 0.01
100 97,2 PALMITIC ACID 0.02
TOTAL 99.99



Chiral test showed there wasn't any synthetic Linalool added
Ratio % Linalool (-) % Linalool (+)
References Mondello 70,8 - 81,5 18,5 - 29,2
NEROLI 78,62 21,38





Below is a scan to @ PPT of a previously stocked Neroil

N.D. (NONE DETECTED)

Data File : C:\HPCHEM\1\DATA\k60721\K607211.D Vial: 2
Acq On : 21 Jul 2006 6:04 pm Operator: ira
Sample : neroli, 60721 Tunisia Inst : GC/MS Ins
Misc : Multiplr: 1.00
Sample Amount: 0.00
MS Integration Params: EVENTS.E
Quant Time: Jul 21 19:17 19106 Quant Results File: KBOIL 100% Pure2LO.RES

Quant Method : C:\HPCHEM\1\METHODS\KBOIL 100% Pure2LO.M (Chemstation Integrator)
Title : Chlorinated benzenes and pesticides
Last Update : Thu Mar 24 15:38:36 2005
Response via : Initial Calibration
DataAcq Meth : KBOIL 100% Pure2LO

Internal Standards R.T. QIon Response Conc Units Dev(Min)
--------------------------------------------------------------------------

System Monitoring Compounds

Target Compounds Qvalue
1) 1,3-Dichlorobenzens 0.00 146 0 N.D.
2) 1,4-Dichlorobenzene 0.00 146 0 N.D.
3) 1,2-Dichlorobenzene 0.00 146 0 N.D.
4) 1,3,5-Trichlorobenzene 0.00 180 0 N.D.
5) 1,2,4-Trichlorobenzene 0.00 180 0 N.D.
6) 1,2,3-Trichlorobenzene 0.00 180 0 N.D.
7) 1,2,3,5-Tetrachlorobenzene 0.00 216 0 N.D.
8) 1,2,4,5-Tetrachlorobenzene 0.00 216 0 N.D.
9) 1,2,3,4-Tetrachlorobenzene 0.00 216 0 N.D.
10) Bromonaphthalene 0.00 127 0 N.D.
11) Pentachlorobenzene 0.00 250 0 N.D.
12) alpha-HCH 0.00 181 0 N.D.
13) Hexachlorobenzene 0.00 284 0 N.D.
14) Atrazin 0.00 200 0 N.D.
15) beta-HCH 0.00 181 0 N.D.
16) gamma-HCH 0.00 181 0 N.D.
17) Heptachlor 0.00 272 0 N.D.
18) delta-HCH 0.00 181 0 N.D.
19) Aldrin 0.00 66 0 N.D.
20) Malathion 0.00 125 0 N.D.
21) Octachlorostyrene 0.00 308 0 N.D.
22) Heptachlor epoxide 0.00 353 0 N.D.
23) o,p'-DDE 0.00 246 0 N.D.
24) Chlordane 0.00 373 0 N.D.
25) p,p'-DDE 0.00 246 0 N.D.
26) o,p'-DDD 0.00 235 0 N.D.
27) Endrin 0.00 81 0 N.D.
28) p,p'-DDD 0.00 235 0 N.D.
29) o,p'-DDT 0.00 235 0 N.D.
30) Endrin aldehyde 0.00 67 0 N.D.
31) p,p'-DDT 0.00 235 0 N.D.
32) Endosulfane sulfate 0.00 272 0 N.D.
33) Methoxychlor 0.00 227 0 N.D.
--------------------------------------------------------------------------

(#) = qualifier out of range (m) = manual integration
K607211.D KBOIL 100% Pure2LO.M Fri Jul 21 19:17:22 2006

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Citrus aurantium
Clasificación científica
Reino: Plantae
División: Fanerógama Magnoliophyta
Clase: Dicotiledónea Magnoliopsida
Subclase: Rosidae
Orden: Sapindales
Familia: Rutaceae
Género: Citrus
Especie: C. aurantium
Nombre binomial
Citrus aurantium
L.

El naranjo amargo (Citrus x aurantium) es un árbol del género Citrus, que forma parte de la familia de las Rutáceas. Muchas variedades de naranja amarga se usan por su aceite esencial, para perfume y saborizante. También como planta medicinal. Otros nombres son naranja agria, naranja bigarade y naranja de Sevilla.

https://es.wikipedia.org/wiki/Citrus_x_aurantium